PROTEUM (and APEX) are the names Bruker uses to describe the instrument control software they write out frames in Bruker format. People publishing an article in a scientific review with any crystal structure from the X-ray service must, at least, cite the « Service de radiocristallographie de la Fédération de Chimie Le Bel FR 2010» as well as the name of the crystallographer who solved the structure.(according to postings on the CCP4BB on by G.

Practical module related to the possession or the management of sealed radioactive sources, electrical devices emitting X-rays and particle accelerators, in the “industry and research” domain.

Theoretical module related to the radiation safety principles and regulations in the « industry and research » domain.

Nathalie Gruber is the Competent Person in Radiation safety (PCR). Please contact the UMR 7140 (team Sylvie Ferlay/Mir Wais Hosseini) and/or the Institut de Physique et de Chimie des Matériaux de Strasbourg (IPCMS) which are competent in these studies and equipped for this type of measurements.

Access to the CSD (Cambridge Structural Database).Īnalyses on powders, thin films, etc…are not performed by the X-ray Service that does not have adequate instruments.

Work stations with structural resolution and refinement programs.

Stereo microscope LEICA M125 equipped with a polarized light device and a video camera EC3 allowing photo capture and crystal visualization in live.

4-circles Bruker APEX II DUO IμS Kappa-CCD diffractometer equipped with two sources (Mo sealed tube and Cu micro-source) and with an Oxford Cryosystem 700 liquid N 2 device for low temperature measurements.4-circles Bruker PHOTON III diffractometer equiped with two micro-sources IμS Mo and IμS Diamond Cu and with an Oxford Cryosystem 800 for low temperature measurements.For researchers with structural resolution and refinement programs, the raw diffraction data can be transferred to them on demand. Only people who learned to use a diffractometer and who are authorized by the person in charge of the crystallography service can make measurements (see “ Convention for the service access“ and “ Procedure for using the Apex II DUO diffractometer“). – XRay Analyses request form (2019) to download – No measurement can be made without this document, the information about the formula and the expected structure is recommended. The Crystallography Service is available to all researchers, regardless of their institute, unit, lab and research team.įill the document and submit it to the X-ray service with the crystals to be studied. The Crystallography Service is in charge of the resolution of molecular structures by single-crystal X-ray diffraction of any compounds, natural or synthetic products. Location: faculty of chemistry, basement

Bruker apex software